《水中揮發酚在線監測儀校準規范》公開征求意見,《水中揮發酚在線監測儀校準規范》公開征求意見-成都市林益源環?？萍加邢薰?/title> <meta name="keywords" content="《水中揮發酚在線監測儀校準規范》公開征求意見" /> <meta name="description" content="2019年11月20日，全國環境化學計量技術委員會發布關于對《水中揮發酚在線監測儀校準規范》(征求意見稿)征求意見的函，向全國各有關單位征求意見。　　主起草單位為北京市計量檢測科學研究院、中節能天融科技有限公司；福建省吉龍德環?？萍加邢薰?、中國環境監測總站、中國環境保護產業協會也參與了起草工作。 ..." /> <link href="/templates/pc_wjdh/css/css.css" rel="stylesheet" type="text/css" /> <link href="/templates/pc_wjdh/css/common.css" rel="stylesheet" type="text/css" /> <script src="/templates/pc_wjdh/js/n/WJDH_common.js"></script> <script type="text/javascript" src="/templates/pc_wjdh/js/n/jquery.qrcode.min.js"></script> <script src="/templates/pc_wjdh/js/n/qrcode.js"></script> <script src="/templates/pc_wjdh/js/n/baidupush.js"></script> <meta name="baidu-site-verification" content="sD1MejEiFv" /> <script src="http://img.dlwjdh.com/upload/saohei/index.js"></script> <meta http-equiv="Cache-Control" content="no-transform" /> <meta http-equiv="Cache-Control" content="no-siteapp" 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style="text-align: justify;">　　2019年11月20日，全國環境化學計量技術委員會發布關于對《水中揮發酚在線監測儀校準規范》(征求意見稿)征求意見的函，向全國各有關單位征求意見。<br>?</div><div style="text-align: justify;">　　主起草單位為北京市計量檢測科學研究院、中節能天融科技有限公司；福建省吉龍德環?？萍加邢薰?、中國環境監測總站、中國環境保護產業協會也參與了起草工作。<br>?</div><div style="text-align: justify;">　　本規范參考了HJ/T 503《水質揮發酚的測定4-氨基安替比林分光光度法》行業標準相關內容，依據JJF 1071《國家計量校準規范編寫規則》、JJF 1001《通用計量術語及定義》和JJF 1059《測量不確定度評定與表示》的規定而制定。<br>?</div><div style="text-align: justify;">　　<strong>一、概述</strong><br>?</div><div style="text-align: justify;">　　水中揮發酚在線監測儀可自動連續監測地下水、地表水、生活污水和工業廢水等水體中揮發酚濃度。<br>?</div><div style="text-align: justify;">　　水中揮發酚在線監測儀測量方法采用4-氨基安替比林(4-AAP)光度法。其原理為水樣中的揮發酚在高溫、酸性環境中蒸餾出來后，pH10.0±0.2介質中，在鐵氰化鉀存在下，與4-氨基安替比林反應顯色，在特定波長處溶液的吸光度與揮發酚含量成正比，以此實現對水中揮發酚的定量分析。儀器主要由進樣單元、反應單元、檢測器單元和數據處理單元組成。<br>?</div><div style="text-align: justify;">　　<strong>二、校準項目和檢定方法</strong><br>?</div><div style="text-align: justify;">　　1、零點漂移<br>?</div><div style="text-align: justify;">　　按照儀器使用說明書要求，待儀器運行穩定后，導入零點校準液，在24h內，每隔1h測定一次，記錄前三次測量的平均值為初始值和每次測量值，取偏離初始值*大的測量值為。按公式(1)計算儀器零點漂移值。<br>?</div><div style="text-align: justify;">　<strong>　三、示值誤差的不確定度評定示例</strong><br>?</div><div style="text-align: justify;">　　1、測量原理<br>?</div><div style="text-align: justify;">　　水樣中的揮發酚在高溫、酸性環境中蒸餾出來后，pH 10.0±0.2介質中，在鐵氰化鉀存在下，與4-氨基安替比林反應顯色，在特定波長510nm處溶液的吸光度與揮發酚含量成正比，以此實現對水中揮發酚的定量分析。<br>?</div><div style="text-align: justify;">　　2、測量方法<br>?</div><div style="text-align: justify;">　　按照儀器使用說明書要求對儀器進行預熱穩定和校準。選用濃度值為量程上限50%的標準溶液，分別重復測量3次，按公式(D.1)計算示值誤差△c。<br>?</div><div style="text-align: justify;">　　3、標準物質、計量設備和校準對象<br>?</div><div style="text-align: justify;">　　標準物質：水中揮發酚成分分析標準物質，相對擴展不確定度優于2%(k=2)。<br>?</div><div style="text-align: justify;">　　計量設備單：標線容量瓶100 mL 、200mL 和1000mL，移液器1mL 和10mL。</div><p class="ai_wjdhcms">本文轉載自環保在線，內容均來自于互聯網，不代表本站觀點，內容版權歸屬原作者及站點所有，如有對您造成影響，請及時聯系我們予以刪除！</p> </div> </div> <div class="adjacent"> <ul> <li>上一篇：<a 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